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  1. 050 理学部
  2. 10 学術雑誌論文
  3. 10 査読済論文
  1. 0 資料タイプ別
  2. 01 学術雑誌論文

Application of biphasic reaction procedure using ferric chloride dissolved in an imidazolium salt and benzotrifluoride (FeIm-BTF procedure) to aza-Prins cyclization reaction

http://hdl.handle.net/10191/31008
http://hdl.handle.net/10191/31008
e1d134cb-bf9c-48c9-9f70-e43274ce4123
名前 / ファイル ライセンス アクション
51_50_6535-6538.pdf 51_50_6535-6538.pdf (311.1 kB)
Item type 学術雑誌論文 / Journal Article(1)
公開日 2014-12-11
タイトル
タイトル Application of biphasic reaction procedure using ferric chloride dissolved in an imidazolium salt and benzotrifluoride (FeIm-BTF procedure) to aza-Prins cyclization reaction
言語
言語 eng
資源タイプ
資源 http://purl.org/coar/resource_type/c_6501
タイプ journal article
著者 Hasegawa, Eietsu

× Hasegawa, Eietsu

WEKO 70

Hasegawa, Eietsu

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Hiroi, Nohara

× Hiroi, Nohara

WEKO 38097

Hiroi, Nohara

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Osawa, Chika

× Osawa, Chika

WEKO 38098

Osawa, Chika

Search repository
Tayama, Eiji

× Tayama, Eiji

WEKO 38099

Tayama, Eiji

Search repository
Iwamoto, Hajime

× Iwamoto, Hajime

WEKO 38100

Iwamoto, Hajime

Search repository
抄録
内容記述タイプ Abstract
内容記述 Aza-Prins cyclization reaction of N-tosyl-3-butenylamine with aliphatic and aromatic aldehydes was performed using a combination of FeCl3 and 1-butyl-3-methylimidazolium hexafluorophosphate (BmimPF6) or 1-butyl-3-methylimidazolium tetrachloroferrate (BmimFeCl4) in benzotrifluoride (BTF). The desired N-tosyl-4-chloro-2-substituted piperidines were obtained from aliphatic aldehydes in comparable yields to those for the previously reported reactions in which FeCl3 was used in CH2Cl2. On the other hand, significant progress for the piperidine synthesis from aromatic aldehydes has been achieved, particularly when BmimFeCl4 was used with FeCl3 in BTF.
書誌情報 Tetrahedron letters
en : Tetrahedron letters

巻 51, 号 50, p. 6535-6538, 発行日 2010-12
出版者
出版者 Elsevier
ISSN
収録物識別子タイプ ISSN
収録物識別子 00404039
書誌レコードID
収録物識別子タイプ NCID
収録物識別子 AA00861801
DOI
識別子タイプ DOI
関連識別子 info:doi/10.1016/j.tetlet.2010.10.018
権利
権利情報 Copyright(C)2010 Elsevier Ltd.
著者版フラグ
値 author
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